Ann is studying acid base neutralization reactions and mixes sodium hydroxide and hydrochloric acid. The reactants were clear, colorless solution and mixing them produces a clear, colorless final solution and the beaker becomes warm. She knows this reaction forms liquid water and an aqueous salt based on the neutralization rules as shown by the chemical equationWhat physical evidence indicates that there has been a chemical reaction NaOH (2q) +HCl (2q) NaCl \ 2Q) +H 2 O (l) A) The solution changes color. B ) Precipitate formation occurs. The beaker changes temperature . D) Gas bubbles form during the reaction.

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely. analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?