Chemistry, 12.11.2020 18:30 ayoismeisalex
These questions are from an experiment where we had a mixture of Ferrocene, acetylferrocene and diacetyl ferrocene and we separated each by using column chromatography. Before doing the column chromatography we did TLC analysis to ensure that we did, in fact, have a mixture of these 3 compounds.
During the column chromatography we first eluted the ferrocene using pure hexane. Then we eluted the acetylferrocene using a 1:1 mixture of hexane and methylene chloride. Then we eluted the diacetylferrocene using a 9:1 mixture of hexane and methylene chloride.
1. Rank ferrocene, acetylferrocene, and diacetylferrocene in order of increasing polarity. Do the TLC results from your fractions support this ranking? Explain.
2. Rank the solvents used in the experiment in order of increasing polarity.
3. Why do you start with the least polar solvent/solvent mixture and progress to increasing polar solvent/solvent mixtures when eluting the ferrocene compounds from the column rather than starting with more polar solvent system and progressing to less polar solvents?
4. How do the thin layer and column chromatography for this experiment compare in regard to stationary and mobile phases?
5. What key feature in the IR spectrum of acetylferrocene distinguishes it from the spectrum of ferrocene?
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