Astudent has performed the grignard reaction between procedure. what composition will have layers after the first extraction with sulfuric acid? phenylmagnesium bromide and methyl benzoate and started the work-up step of the the top layer after the extraction with sulfuric acid contains choose and sulfuric acid tion the bottom layer after the extraction with sulfuric acid diphenyl ketone, phenylmagnesium bromide, mag magnesium salts, sulfuric acid phenyl magnesium bromide, small amount of water, and sulfuric acid triphenyl methanol, small amount of water, and sulfuric acld contains

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely. analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?

How many moles of sulfur dioxide are produced when 4.38 moles of oxygen completely react with iron (iv) sulfide

In a copper wire, a temperature increase is the result of which of the following